2-[(6-Bromo-2-pyridyl)amino]pyridineN-oxide

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2-[(6-Bromo-2-pyrid­yl)amino]pyridine N-oxide

In the crystal structure of the title compound, C(10)H(8)BrN(3)O, the dihedral angle between the two pyridine rings is 2.48 (2)°. A weak intramolecular N-H⋯O hydrogen bond is present.

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6-Bromo-2-naphthol–piperazine (2/1)

In the title compound, 2C(10)H(7)BrO·C(4)H(10)N(2), the piperazine (pip) mol-ecule displays a chair conformation and is linked to two mol-ecules of 6-bromo-2-naphthol (bno) via O-H⋯N hydrogen bonds. Weak N-H⋯O hydrogen bonds from pip to bno mol-ecules result in chains propagating in [100]. The chains inter-act via C-H⋯π inter-actions.

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In the title compound, C(21)H(18)BrN(2)O(5)P, the six-membered oxaza-phosphinine ring is in a twist-boat conformation. One of the phosphoryl O atoms is in an equatorial configuation while the other is axial with respect to the oxaza-phosphinine ring. The mean planes of the benzene ring to which the nitro group is attached and the phenyl ring form a dihedral angle of 83.5 (1)°. In the crystal st...

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5-Bromo-2-methyl­pyridine N-oxide

In the mol-ecule of the title compound, C(6)H(6)BrNO, the methyl C and oxide O atoms lie in the pyridine ring plane, while the Br atom is displaced by 0.103 (3) Å. In the crystal structure, inter-molecular C-H⋯O hydrogen bonds link the mol-ecules into centrosymmetric dimers.

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The title compound, C(13)H(15)BrClNO, was prepared by the condensation of equimolar quanti-ties of 3-bromo-5-chloro-salicyl-aldehyde with cyclo-hexyl-amine in methanol. There is an intra-molecular O-H⋯N hydrogen bond in the mol-ecule. The cyclo-hexyl ring adopts a chair conformation.

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2008

ISSN: 1600-5368

DOI: 10.1107/s1600536808022058